Crystalline compound I demonstrated? (6)
I believe the answer is:
isatin
'crystalline compound' is the definition.
'i demonstrated?' is the wordplay.
'demonstrated?' becomes 'satin' (as in held a sit-in, a kind of demonstration).
'i'+'satin'='ISATIN'
(Other definitions for isatin that I've seen before include "chemical derived from indigo" , "Dye ingredient" , "compound" .)