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Test (5)

Ross

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4

5

2.6 3,3

'test' is the definition.
(synonyms)

This is the entire clue.

(Other definitions for assay that I've seen before include "Test (a metal or ore)" , "Test(ing) of a substance, such as precious metal" , "metallurgical test" , "Test quality of metals" , "'Analyse, precious metal, say (5)'" .)

I've seen this clue in The Star Tribune, the Penny Press, The Mirror, The Times, the Sydney Morning Herald and the Evening Standard.
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